>>62
Well, I'm shit. Sorry for the goddamn wait. I'm going to try to describe this synthesis as best as I can. Be forewarned that the highly critical step of washing and recrystallizing the ETN, as I already mentioned, is omitted. Ideally you want to stabilize your end product in the following order: Wash with water (quite a bit), wash with baking soda solution for a while, seperate out the baking soda, dissolve your ETN in something (acid is trapped inside the crystals, that's bad and will degrade your batch over time. If it starts yellowing your ETN needs help, stat, to keep up a shelflife), recrystallize it by crashing it into cool water with a tad of baking soda, and then drying it. This is a VERY rough description of how it goes. There are a lot of various techniques for each individual step and if you really want to understand them I'm not qualified to explain them IMO, for now.
I will also warn you, your yields from this process will be shit. This is not a very exact method, it was a spitball based on other procedures that got meh yields. Expect a yield of 10-20 grams, IF you are lucky. This is a proof of concept.
ALSO. Do not fucking try to skim this shit or read along as you do it. Read it through entirely twice, then make a cheat sheet to have with you in your lab.
So, lets start. You're going to need some of pic related coffee sweetener. Why? Is this magical good stuff? No. This shit was the best I could find in my local grocery store. You can and should try to do better. Unless you're lazy, like me. To be exact, you're going to be using 35 grams of this shit. You will probably want to grind it up so it's significantly finer than you start with. it's not as fine as you might like out of the box.
The other thing you'll need, is ammonium nitrate. You can get this out of cold packs, the ones with water that you smack to make cold. Just trim the corner open, and take the prills out. You'll need about 100 grams of this shit. And you'll be wanting to grind it up. You can probably get away with less, but eh, AN is cheap as hell, the annoying part is grinding it up in a mortarPost too long. Click here to view the full text.
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